Patent application number | Description | Published |
20100095602 | TECHNIQUES AND MATERIALS FOR THE ACCELERATED REMOVAL OF CATALYST MATERIAL FROM DIAMOND BODIES - A method for making a thermally stable cutting element may include forming an acid mixture containing two different acid species by combining an acid solution and at least one acid-forming compound, wherein the at least one acid-forming compound is provided in solid form, and wherein the at least one acid-forming compound produces an acid that is different than the acid solution; treating at least a portion of a sintered diamond body by placing the sintered diamond body in the acid mixture, wherein the sintered diamond body comprises: a matrix phase of bonded-together diamond grains; a plurality of interstitial regions dispersed within the matrix phase; and a metal material disposed within a plurality of the interstitial regions; wherein the treating removes the metal material from at least a portion of the plurality of interstitial regions; and removing the sintered diamond body from the acid mixture after a predetermined length of time, wherein at least a portion of the diamond body removed from the acid mixture is substantially free of the metal material and is a thermally stable diamond body. | 04-22-2010 |
20110036643 | THERMALLY STABLE POLYCRYSTALLINE DIAMOND CONSTRUCTIONS - Thermally stable polycrystalline constructions comprise a diamond body joined with a substrate, and may have a nonplanar interface. The construction may include an interlayer interposed between the diamond body and substrate. The diamond body preferably has a thickness greater than about 1.5 mm, and comprises a matrix phase of bonded together diamond crystals and interstitial regions disposed therebetween that are substantially free of a catalyst material used to sinter the diamond body. A replacement material is disposed within the interstitial regions. A population of the interstitial regions may include non-solvent catalyst material and/or an infiltrant aid disposed therein. The diamond body comprises two regions; namely, a first region comprising diamond grains that may be sized smaller than diamond grains in a second region, and/or the first region may comprise a diamond volume that is greater than that in the second region. | 02-17-2011 |
20110052803 | Method of Forming Metal Deposits on Ultrahard Materials - A method of forming a metal deposit on an ultra-hard material. In an embodiment, the method includes providing a plurality of ultra-hard particles, mixing the ultra-hard particles in a solution with a metal salt, drying the solution to create a mixture of metal salt particles adhered to surfaces of the ultra-hard particles, heating the mixture to convert the metal salt particles into metal deposits on the surfaces of the ultra-hard particles, and HTHP sintering the mixture of ultra-hard particles with the metal deposits to form a polycrystalline ultra-hard material. | 03-03-2011 |
20120055099 | EDM CUTTABLE, HIGH CBN CONTENT SOLID PCBN COMPACT - The present disclosure relates to cubic boron nitride (cBN) cutting elements that have high cBN content and that are cuttable by electric discharge machining (EDM). A cutting element according to an embodiment includes a self-sintered polycrystalline cubic boron nitride (PCBN) compact, having a first phase of cubic boron nitride (cBN) particles and a ceramic binder phase with titanium compounds. The first phase occupies greater than 80% by volume of the self-sintered PCBN compact. The self-sintered PCBN compact has an electrical conductivity sufficient to be cuttable by electrical discharge machining. | 03-08-2012 |
20120131856 | FABRICATION OF ULTRAFINE POLYCRYSTALLINE DIAMOND WITH NANO-SIZED GRAIN GROWTH INHIBITOR - The present disclosure relates to the formation of polycrystalline diamond materials with fine diamond grains and nano-sized particles of a grain growth inhibitor. In one embodiment, a method of fabricating a polycrystalline diamond material is provided. The method includes providing a mixture of diamond particles with an average particle size of about 1 micron or less, distributing a plurality of nano-sized titanium-containing particles with the diamond mixture, to act as a grain growth inhibitor, and sintering the mixture of diamond particles and titanium-containing particles at high pressure and high temperature to create a polycrystalline structure of sintered diamond grains. The sintered diamond grains have an average size of about 1 micron or less. | 05-31-2012 |
20130084446 | HIGH CONTENT PCBN COMPACT INCLUDING W-RE BINDER - The present invention relates to tungsten-rhenium coated compounds, materials formed from tungsten-rhenium coated compounds, and to methods of forming the same. In embodiments, tungsten and rhenium are coated on ultra hard material particles to form coated ultra hard material particles, and the coated ultra hard material particles are sintered at high temperature and high pressure. | 04-04-2013 |
20130152480 | METHODS FOR MANUFACTURING POLYCRYSTALLINE ULTRA-HARD CONSTRUCTIONS AND POLYCRYSTALLINE ULTRA-HARD CONSTRUCTIONS - Polycrystalline ultra-hard constructions are made by subjecting a sintered ultra-hard body, substantially free of a sintering catalyst material, to a further HPHT process. The process is controlled to initially melt and infiltrating a filler material into the sintered ultra-hard body to form a filler region having interstitial regions filled with the filler material. The filler region extends a partial depth into the sintered ultra-hard body and is formed at a temperature below the melting temperature of an infiltrant material. Next, the process is controlled to melt and infiltrate the infiltrant material into the sintered ultra-hard body to form an infiltrant region that extends a partial depth into the sintered ultra-hard body. A portion of the filler region and/or the infiltrant region may be removed to form a thermally stable region. | 06-20-2013 |
20130168156 | DIAMOND ENHANCED INSERT WITH FINE AND ULTRAFINE MICROSTRUCTURE OF PCD WORKING SURFACE RESISTING CRACK FORMATION - An insert for a drill bit may include a metallic carbide body; an outer layer of polycrystalline diamond material on the uppermost end of the insert, wherein the polycrystalline diamond material comprises: a plurality of interconnected diamond grains; a plurality of additive grains; a binder material; wherein the average additive grain size is smaller than the average diamond grain size. | 07-04-2013 |
20130168158 | METHOD FOR BRAZE JOINING OF CARBONATE PCD - A method for making a diamond compact includes pre-heating a diamond body which includes a carbonate catalyst to convert at least a portion of the carbonate catalyst into an oxide, assembling the diamond body and a substrate, providing a braze material between the diamond body and the substrate to form a diamond compact, heating the braze material to melt the braze material and form a braze joint between the diamond body and the substrate, and cooling the braze material after increasing the pressure. A bit having a diamond compact including a carbonate catalyst and a metal oxide mounted thereon. | 07-04-2013 |
20130263748 | HIGH PRESSURE HIGH TEMPERATURE CELL - A high-pressure high-temperature cell including two or more thermal insulation layers is described. A high-pressure high-temperature cell including a current path through a thermal insulation layer, the current path being electrically connected to a heating element and having an indirect path through the thermal insulation layer, is also described. High-pressure high-temperature press systems including the foregoing the high-pressure high-temperature cells alone or in combination are also disclosed. | 10-10-2013 |
20130266678 | THERMAL INSULATION LAYER AND PRESSURE TRANSFER MEDIUM FOR HIGH PRESSURE HIGH TEMPERATURE CELL - A thermal insulation layer for an HPHT cell, the thermal insulation layer including CsCl, CsBr, CsI, or a combination thereof, and the thermal insulation layer being electrically insulating; the thermal insulation layer including a thermal insulation sleeve and/or a thermal insulation button for an HPHT cell; a pressure transfer medium for an HPHT cell, the pressure transfer medium including CsBr, CsI or a combination thereof; and a pressure transfer medium for an HPHT cell, the pressure transfer medium including CsCl and additive, with the proviso that the additive does not include ZrO | 10-10-2013 |
20130298475 | EDM CUTTABLE, HIGH CBN CONTENT SOLID PCBN COMPACT - The present disclosure relates to cubic boron nitride (cBN) cutting elements that have high cBN content and that are cuttable by electric discharge machining (EDM). A cutting element according to an embodiment includes a self-sintered polycrystalline cubic boron nitride (PCBN) compact, having a first phase of cubic boron nitride (cBN) particles and a ceramic binder phase with titanium compounds. The first phase occupies greater than 80% by volume of the self-sintered PCBN compact. The self-sintered PCBN compact has an electrical conductivity sufficient to be cuttable by electrical discharge machining. | 11-14-2013 |
20140007512 | TECHNIQUES AND MATERIALS FOR THE ACCELERATED REMOVAL OF CATALYST MATERIAL FROM DIAMOND BODIES - A method for making a thermally stable cutting element may include forming an acid mixture containing two different acid species by combining an acid solution and at least one acid-forming compound, wherein the at least one acid-forming compound is provided in solid form, and wherein the at least one acid-forming compound produces an acid that is different than the acid solution; treating at least a portion of a sintered diamond body by placing the sintered diamond body in the acid mixture, wherein the sintered diamond body comprises: a matrix phase of bonded-together diamond grains; a plurality of interstitial regions dispersed within the matrix phase; and a metal material disposed within a plurality of the interstitial regions; wherein the treating removes the metal material from at least a portion of the plurality of interstitial regions; and removing the sintered diamond body from the acid mixture after a predetermined length of time, wherein at least a portion of the diamond body removed from the acid mixture is substantially free of the metal material and is a thermally stable diamond body. | 01-09-2014 |
20140013913 | THERMALLY STABLE PCD WITH PCBN TRANSITION LAYER - The present disclosure relates to cutting tools incorporating polycrystalline diamond bodies used for subterranean drilling applications, and more particularly, to a thermally stable polycrystalline diamond body joined to a substrate to form a cutting element. The thermally stable polycrystalline diamond body may be binderless polycrystalline diamond or a non-metal catalyst polycrystalline diamond. A polycrystalline cubic boron nitride layer is also provided, bonded on one side to the polycrystalline diamond body and on the other side to the substrate. | 01-16-2014 |
20140130418 | METHOD OF MAKING CARBONATE PCD AND SINTERING CARBONATE PCD ON CARBIDE SUBSTRATE - A method of forming a polycrystalline diamond body includes mixing a sintering agent with diamond powder to form a premixed layer, the sintering agent including at least one alkaline eat mewl carbonate; forming an infiltration layer adjacent to the premixed layer, the infiltration layer including an infiltrant material including at least one alkaline earth metal carbonate; and subjecting the premixed layer and the infiltration layer to high pressure high temperature conditions. | 05-15-2014 |
20140131117 | SINTERING OF THICK SOLID CARBONATE-BASED PCD FOR DRILLING APPLICATION - A method of making a polycrystalline diamond compact includes forming multiple layers of premised diamond particles and carbonate material, where the carbonate material includes an alkaline earth metal, carbonate, and where each layer has a weight percent ratio of diamond to carbonate that is different from adjacent layers. The layers are subjected to high pressure high temperature conditions to form polycrystalline diamond. | 05-15-2014 |
20140259962 | CARBONATE PCD WITH A DISTRIBUTION OF Si AND/OR Al - A method for making a carbonate polycrystalline diamond body includes combining a first quantity of diamond with a first quantity of magnesium carbonate to form a first layer for forming a working surface, and combining a second quantity of magnesium carbonate to form a second layer adjacent to the first layer, forming an assembly. The method includes placing a quantity of silicon or aluminum in or adjacent to at least a portion of the assembly and sintering the assembly including the silicon or aluminum at high pressure and high temperature, causing the silicon or aluminum to infiltrate at least one layer of the assembly. | 09-18-2014 |
20140259963 | CARBONATE PCD AND METHODS OF MAKING THE SAME - A polycrystalline diamond body, and a method for making a carbonate polycrystalline diamond body includes combining a first quantity of diamond particles with a first quantity of magnesium carbonate to form a first layer in an enclosure, the first layer having a working surface, and placing a second quantity of magnesium carbonate in the enclosure forming a second layer, the first layer and the second layer forming an assembly. A quantity of at least one of silicon or aluminum is mixed in with or placed adjacent to at least one of the first layer or the second layer. The assembly, including the at least one of silicon or aluminum, is sintered at high pressure and high temperature, causing the at least one of silicon or aluminum to infiltrate at least one layer of the assembly, forming a polycrystalline diamond body. | 09-18-2014 |
20150068817 | THERMALLY STABLE POLYCRYSTALLINE DIAMOND AND METHODS OF MAKING THE SAME - A method of making a cutting element includes subjecting a mixture of diamond particles and a carbonate material to high-pressure high-temperature sintering conditions to form a sintered carbonate-polycrystalline diamond body having a diamond matrix of diamond grains bonded together and carbonates residing in the interstitial regions between the diamond grains, the carbonate material having a non-uniform distribution throughout the diamond matrix. The carbonate-polycrystalline diamond body is subjected to a controlled temperature, a controlled pressure condition or a combination thereof, to effect an at least partial decomposition of the carbonate material. | 03-12-2015 |