Patent application number | Description | Published |
20090166180 | PROCESS FOR PRODUCING ISOCYANATES - An isocyanate is produced by: | 07-02-2009 |
20090209784 | Process for the preparation of isocyanates - The present invention relates to a process for the preparation of isocyanates by reacting the appropriate amines with phosgene, condensing the gas mixture thereby obtained, stripping the liquid phase thereby obtained and returning the solvent so retained in liquid form to the reaction stage. The gaseous constituents are then purified further in an absorption process. | 08-20-2009 |
20100152484 | PROCESS FOR THE PREPARATION OF ISOCYANATES IN THE GAS PHASE - Aromatic isocyanates are produced by reacting one or more aromatic primary amines with phosgene in the gas phase. The phosgene and primary aromatic amine(s) are reacted at a temperature above the boiling temperature of the amine(s) in a reactor having a reaction space which is essentially rotationally symmetric to the direction of flow. The flow fate, averaged over the cross-section, of the reaction mixture along the axis of the essentially rotationally symmetric reaction space in the section of the reaction space in which the conversion of the amine groups into isocyanate groups is between 4 and 80 % is not more than 8 m/sec. The flow rate averaged over the cross-section of the reaction mixture along the axis of the essentially rotationally symmetric reaction space in the section of the reaction space in which the conversion of the amine groups into isocyanate groups is 4 to 80 % is always below the flow rate averaged over the cross-section at the start of this section. | 06-17-2010 |
20100160674 | PROCESS FOR THE PREPARATION OF ISOCYANATES IN THE GAS PHASE - Meta-toluene-diisocyanate is produced by reacting meta-toluenediamine with phosgene in the gas phase. The meta-toluenediamine to be vaporized for use in this phosgenation process must contain less than 0.5 wt. % of toluenediamine residue, a total of less than 0.2 wt. % of ammonia and cycloaliphatic amines, and less than 20 ppm of heavy metals. At least 0.1 wt. % of the liquid meta-toluenediamine being to be vaporized must not be vaporized. This non-vaporized content of the meta-toluenediamine must not be fed to the phosgenation reactor. | 06-24-2010 |
20110021811 | PROCESS FOR THE PREPARATION OF TOLUENE-DIISOCYANATE - The present invention relates to a process for the preparation of toluene-diisocyanate. In this process, toluenediamine is reacted with phosgene to give crude toluene-diisocyanate, the crude toluene-diisocyanate is purified by distillation, the distillation residue formed during the distillation is hydrolysed at temperatures of less than 230° C. under absolute pressures of less than 30 bar, and the toluenediamine formed by this process is subsequently recycled into the reaction of toluenediamine and phosgene. | 01-27-2011 |
20120108845 | PROCESS FOR THE PREPARATION OF ISOCYANATES IN THE GAS PHASE - Isocyanates are produced by reacting a primary amine with phosgene in the gas phase. In this process, the amine is vaporized and then superheated prior to introduction into the reactor. The amine is superheated to a temperature at least 10° C. above dew point before entry into the reactor. A pressure difference between the vaporizer and entry into the reactor of from 1 to 500 mbar is maintained. | 05-03-2012 |
20120123152 | PROCESS FOR THE PREPARATION OF ISOCYANATES - An isocyanate is produced by reacting an amine with a stoichiometric excess of phosgene in the gas phase. This reaction is carried out at a temperature above the amine's boiling point to obtain a liquid stream containing the isocyanate and a gas stream containing hydrogen chloride and phosgene. The gas stream containing hydrogen chloride and phosgene thus produced is separated into a gas stream containing hydrogen chloride and a liquid stream containing phosgene. At least part of the liquid stream containing phosgene is then converted to a gas stream containing phosgene which gas stream is then recycled. The gaseous phosgene stream is maintained at a higher pressure than the liquid phosgene stream. | 05-17-2012 |
20120289745 | METHOD FOR PRODUCING AROMATIC AMINES IN THE LIQUID PHASE - The invention relates to a process for the preparation of aromatic amines in the liquid phase by catalytic hydrogenation of the corresponding nitroaromatic compounds in at least two reaction spaces connected in series, wherein at least one reaction space is operated isothermally and at least the reaction space connected downstream thereof is operated adiabatically, and in preferred embodiments the sudden adiabatic temperature change is used for monitoring the reaction. | 11-15-2012 |
20120302785 | METHOD FOR PRODUCING ISOCYANATES IN THE GAS PHASE - An isocyanate is produced by continuously reacting an amine with phosgene in the presence of an inert substance in the gas phase. In this process, a phosgene-containing stream and a stream containing both the amine and the inert substance are fed into a reactor. The molar ratio of the inert substance to the amino groups in the stream is greater than 0 but less than 45 mol %. This molar ratio changes by no more than 99% during a 20 minute period. | 11-29-2012 |
20130131377 | METHOD FOR PRODUCING ISOCYANATES IN THE GAS PHASE - The invention relates to a process for the preparation of isocyanates by reaction of the corresponding amines with phosgene in the gas phase, wherein a diluent containing between 90.0000% by weight and 99.9999% by weight of substances which are inert in the phosgenation process and between 0.0001% by weight and 10.0000% by weight of oxygen is present during the conversion of the amine into the gas phase and the molar ratio of amine to oxygen (O | 05-23-2013 |
Patent application number | Description | Published |
20090324938 | CONDUCTIVE, ORGANIC COATINGS WITH LOW LAYER THICKNESS AND GOOD PLASTICITY - The invention relates to a metal sheet, or a component made of a metallic material, comprising a layer system on the surface with at least the following layers: a) a conversion layer, comprising no more than 1 mg chromium per m | 12-31-2009 |
20090324957 | CONDUCTIVE, ORGANIC COATINGS HAVING AN OPTIMIZED POLYMER SYSTEM - A substance for coating metal surfaces, comprising organic resin components that are dissolved or dispersed in an organic solvent, or solvent mixture, having at least the following organic resin components: a) epoxy resin, present as polyether comprising hydroxyl groups, based on a bisphenol epichlorohydrin polycondensation product, b) blocked aliphatic polyisocyanate, c) unblocked aliphatic polyisocyanate, d) at least one reaction component, selected from polyesters comprising hydroxyl groups and poly(meth)acrylates comprising hydroxyl groups. The substance may also comprise at least one conductivity pigment. The invention further provides a method for coating a sheet metal with this substance, the respectively coated sheet metal, and the use thereof. | 12-31-2009 |
20090324983 | COMPOSITION AND PROCESS FOR COATING METAL SURFACES - A composition for coating metal surfaces based on crosslinking polyester resins as an organic constituent, which, based on its total mass, contains from 4 to 20% by weight of aluminum flakes and not more than 0.1% by weight of compounds containing isocyanate groups. The composition preferably comprises, as an organic binder, at least one hydroxylated polyester resin, preferably having a mean molar mass in the range from 2000 to 15,000, a crosslinking component for the hydroxylated polyester resin and an acidic crosslinking catalyst. A process for applying the composition to metal strip in a belt process is likewise disclosed. The layer application is adjusted within the range from 3 to 30 μm according to the end use, for which double coating may be advantageous. For example, the composition may serve as a “galvanization replacement”. | 12-31-2009 |
20100209732 | PRELIMINARY METALLIZING TREATMENT OF ZINC SURFACES - The invention relates to a method for a preliminary metallizing treatment of galvanized or zinc alloy-coated steel surfaces or joined metallic parts that at least partly have zinc surfaces, in a surface treatment encompassing several process steps. In the disclosed method, metallic coats of especially a maximum of 100 mg/m | 08-19-2010 |