| Class / Patent application number | Description | Number of patent applications / Date published |
|---|
| 560248000 | Purification or recovery | 17 |
| 20090076298 | Utilization of acetic acid reaction heat in other process plants - Integrated processes and systems for producing acetic acid and vinyl acetate are provided. In the processes and systems, a portion of the heat produced during the production of the acetic acid is transferred to the vinyl acetate production and/or purification process and system to facilitate production and/or purification of the vinyl acetate product. The process and systems described herein are useful in conjunction with any of the various known processes for the production of acetic acid and vinyl acetate. The heat of the acetic acid production reaction may be transferred to the vinyl acetate production system by any suitable heat transfer processes and systems. The heat may be provided to the purification section at a variety of locations in the vinyl acetate production and purification systems, depending on the specific configuration of the system to which the processes and systems. The process and systems described herein are useful to provide cost and energy savings in vinyl acetate production processes. | 03-19-2009 |
| 20090131711 | SINGLE-STAGE ESTERIFICATION OF OILS AND FATS - A process for producing alkyl esters useful as bio-fuels and/or lubricants. An alkyl ester product produced by the process. The process comprises a single-stage reaction for esterifying a de-watered glyceride-containing feedstock with an anhydrous short chain alcohol in the presence of a basic esterification catalyst to produce a reaction product comprising alkyl esters and a reaction by-product comprising glycerol-containing substances and the catalyst-containing alcohol. The single-stage esterification reaction is conducted within a temperature and negative-pressure controllable vessel. The alkyl ester product is separated from the re-action by-product and may be further de-watered and/or purified. The catalyst-containing alcohol may be separated from the reaction by-product, de-watered and reused. The glycerol-containing substances may be separated from the reaction by-product and further purified. Useful glyceride-containing feedstocks include those prepared from plant or animal or fish materials, particularly those produced from seeds of mustard, canola, soybean, corn, cotton, flax and palm. | 05-21-2009 |
| 20090198083 | Method for manufacturing esters from acid and system thereof - A process for manufacturing esters from acid and alcohol and a system thereof are provided, wherein the system includes a reactive distillation column, a sidestream reactor packed with catalyst, and a decanter for conducting the method. The method is carried out by (a) extracting a first mixture of acid and alcohol from the reactive distillation column, for then feeding the first mixture to at least one sidestream reactor packed with catalyst to obtain a reaction product; (b) feeding the reaction product from the sidestream reactor to the reactive distillation column, allowing a second mixture of alcohol, ester and water to be separated from a top end of the reactive distillation column; (c) feeding the second mixture into the decanter to separate an organic phase from an aqueous phase; and (d) separating esters from the organic phase. The method and system allow the esters to be extracted without using a plurality of recovering columns and decanters, and are capable of improving packing/changing catalyst in a single reactive distillation column. | 08-06-2009 |
| 20100305355 | METHOD OF REMOVING HEAVY HYDROCARBONS FROM REACTION PRODUCTS IN THE PRODUCTION OF SEC-BUTYL ACETATE - The present invention relates to a method of removing heavy hydrocarbon from reaction products in producing sec-butyl acetate, characterized in that the method comprises: drawing out materials from the enrichment area of the heavy hydrocarbon; contacting the materials with water sufficiently to make the heavy hydrocarbon in materials and the water stratify naturally wherein the heavy hydrocarbon is contained in the upper layer and the water is contained in the lower layer; and discharging the upper layer and recycling the lower layer into the system. The enrichment area of heavy hydrocarbon refers to the area enriched with heavy hydrocarbon and formed in the bottom of an azeotropic distillation tower during the process of azeotropic separation, while the process of azeotropic separation refers to a process of feeding the mixture of sec-butyl acetate, acetate acid and heavy hydrocarbon into the azeotropic distillation tower and adding azeotropic agent into the azeotropic distillation tower to conduct azeotropic distillation, then evaporating the azeotropic mixture formed by sec-butyl acetate and azeotropic agent from the top of the azeotropic distillation tower, and meanwhile, the acetic acid and the heavy hydrocarbon falling into the bottom of the tower. | 12-02-2010 |
| 20110137074 | PROCESS FOR THE PRODUCTION OF ACETIC ACID ETHYLENE AND VINYL ACETATE MONOMER - An integrated process for the production of acetic acid, ethylene and vinyl acetate monomer comprising the steps of:
| 06-09-2011 |
| 20110144378 | CATALYTIC REACTION-RECTIFICATION INTEGRATED PROCESS AND SPECIALIZED DEVICE THEREOF - A catalytic reaction-rectification integrated process and a catalytic reaction-rectification integrated column (T- | 06-16-2011 |
| 20110190531 | PROCESS FOR PRODUCING AN ETHYL ACETATE SOLVENT AND CO-PRODUCTION OF ETHANOL - Recovery of an ethyl acetate solvent, optionally with the recovery of ethanol, from a crude product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude product are employed to allow recovery of the ethyl acetate solvent. | 08-04-2011 |
| 20110190532 | PROCESS FOR PRODUCING AN ESTER FEED STREAM FOR ESTERS PRODUCTION AND CO-PRODUCTION OF ETHANOL - Recovery of an ester feed stream, optionally with the recovery of ethanol, from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude ethanol products are employed to allow recovery of the ester feed stream and for integration of the ester feed stream with an esters production process. The composition of the ester feed stream may vary, but at least comprises ethyl acetate and ethanol. The ester feed stream may be fed to one or more locations within the esters production process depending on the composition of the ester feed stream. | 08-04-2011 |
| 20110257427 | PURIFICATION OF CARBOXYLIC ESTERS BY EXTRACTIVE DISTILLATION - In a process for purifying carboxylic esters such as ethyl formate, a carboxylic ester to be purified is distilled in the presence of an extractant, preferably by (a) allowing vapor of the carboxylic ester to be purified to ascend in a distillation column; (b) conveying the extractant in countercurrent to the vapor in an extractive distillation column; (c) taking off pure carboxylic ester above the extractive distillation zone. The extractant is, for example, selected from among diols, polyols, open-chain or cyclic amides. | 10-20-2011 |
| 20120083622 | METHOD AND APPARATUS FOR PREPARING AN ESTER - A method for preparing an ester is provided. The method includes steps of mixing an acid and an alcohol in a reactive distillation column to generate a first gas mixture; transporting the first gas mixture out of the reactive distillation column; cooling down the first gas mixture for a phase separation to obtain a first liquid mixture in an upper phase; transporting the first liquid mixture back to the reactive distillation column; obtaining a second liquid mixture at a middle section of the reactive distillation column; transporting the second liquid mixture to a separative distillation column; and obtaining the ester at a bottom section of the separative distillation column. | 04-05-2012 |
| 20120136170 | PROCESS FOR THE MANUFACTURING OF VINYL ACETATE - The present invention relates to a process for the separation of vinyl acetate from a gas mixture formed by the reaction of ethylene with acetic acid and oxygen in the gas phase over catalysts comprising palladium or palladium compounds. | 05-31-2012 |
| 20120277463 | Extractive Distillation of Crude Alcohol Product - Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid using an extractive distillation column. The column yields a first residue that comprises ethanol, ethyl acetate, acetic acid, and water. The first residue is separated in a second column to yield a second distillate comprising ethanol and ethyl acetate. The second distillate is then separated in a third column to yield a third distillate comprising ethyl acetate and a third residue comprising ethanol. | 11-01-2012 |
| 20130018203 | METHOD FOR PRODUCING N-PROPYL ACETATE AND METHOD FOR PRODUCING ALLYL ACETATEAANM Oguchi; WataruAACI Kawasaki-shiAACO JPAAGP Oguchi; Wataru Kawasaki-shi JPAANM Maruta; HiroshiAACI Oita-shiAACO JPAAGP Maruta; Hiroshi Oita-shi JP - Provided is a method for producing n-propyl acetate, which is capable of obtaining high-purity allyl acetate with a low amount of coexisting water and is capable of producing n-propyl acetate with a high yield. The method includes an extraction process of subjecting a raw material liquid containing allyl acetate and water to an extraction operation using water as an extraction solvent and separating the extract into an oily phase and an aqueous phase, a distillation process of distilling the oily phase to obtain a distillate containing allyl acetate as a main component, and a hydrogenation process of subjecting the distillate to a hydrogenation reaction. | 01-17-2013 |
| 20130131376 | METHOD FOR PRODUCING A CARBOXYLIC ACID ESTER - A method for producing a carboxylic acid ester is described, particularly an acetic acid ester and specifically an ethyl acetate ester. Also described, is a method by which a carboxylic acid ester goes from an organic phase produced from an esterification reaction between a carboxylic acid and an alcohol. The organic phase can include, at least predominantly, the carboxylic acid ester and also minor amounts of alcohol and water. Further described, is a separation step, during which the organic phase is depleted of alcohol and free of carboxylic acid via a liquid-liquid extraction operation that is performed by placing said organic phase in contact with an aqueous phase, thus enabling the alcohol and the carboxylic acid, that are present in the organic phase, to be extracted to the aqueous phase. | 05-23-2013 |
| 20130331601 | METHOD FOR RECOVERY OF ORGANIC ACID FROM DILUTE AQUEOUS SOLUTION - The present invention relates to a method and an arrangement for recovery of at least one organic acid from a dilute aqueous solution thereof. In this method a complex between said organic acid and an extractant is formed by contacting the solution with a reactive extractant and dissolving the formed complex into said extractant thus forming an extractant phase. The organic acid is removed from the formed complex by esterification using an alcohol. | 12-12-2013 |
| 20140155648 | Manufacture of a Triiodinated Contrast Agent - A new compound, (S)-5-(2-acetoxypropanamido)-2,4,6-triiodoisophthalic acid, of formula II (S)-5-(2-acetoxypropanamido)-2,4,6-triiodoisophthalic acid. Said new compound is of use for the production of triiodinated contrast agent, especially lopamidol, with low content of acetyl and hydroxyacetyl analogs. The new compound may be formed from 5-amino-2,4,6-triiodoisophtalic acid by acylating with (S)-1-chloro-1-oxopropan-2-yl acetate. The new compound may then be converted to the respective acid dichloride by reacting with a chlorinating reagent, which is a further object of the present invention, followed by the amidation with 2-amino-1,3-propanediol and acetate hydrolysis. | 06-05-2014 |
| 20140323757 | Biosurfactant Isolated from Yeast - The present invention provides a novel compound isolated from yeasts and its use as a bio-surfactant. The bio-surfactant of the present invention shows high surfactant activity, is biodegradable, and is safe to the human body due to its low toxicity. Also, the bio-surfactant of the present invention can be eco-friendly produced through a cultivation of a microorganism in large quantities. | 10-30-2014 |
