Patent application number | Description | Published |
20090061349 | LOW MELT TONERS AND PROCESSES THEREOF - A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the T | 03-05-2009 |
20090123864 | Ultra Low Melt Toners Comprised of Crystalline Resins - A toner having an amorphous resin, a crystalline resin, and a colorant, wherein the crystalline resin has a melting temperature of at least 70° C. and a recrystallization point of at least 47° C. exhibits improved document offset properties and improved heat cohesion. Annealing the toner further improves the heat cohesion and morphology of the toner. | 05-14-2009 |
20090142692 | LOW MOLECULAR WEIGHT LATEX AND TONER COMPOSITIONS COMPRISING THE SAME - Provided are a latex process and a toner process, both of which include the preparation of a latex having weight average molecular weight of from about 12×10 | 06-04-2009 |
20090246679 | TONER PROCESS - The present disclosure provides processes for preparing toner particles, in which fewer coarse particles are generated. The process includes introducing a buffer solution during coalescence of the toner slurry. The amount of coarse particles in the resulting toner particles may, in embodiments, be reduced to less than about 5 percent by weight of the total toner particles generated. | 10-01-2009 |
20100021841 | LOW MELT TONERS AND PROCESSES THEREOF - A process for preparing toner particles and compositions adapted for use in preparing toners that comprise a blend of a first polyester resin with a second sharp melting polyester resin. The process includes forming an emulsion resin comprising a branched polyester resin, a crystalline polyester resin, a colorant, and optionally a wax. The resin mixture is aggregated using an aggregating agent, such as a zinc acetate solution, to form an aggregate mixture. The aggregate mixture is then coalesced at a temperature of from about 5 to about 20° C. above the T | 01-28-2010 |
20100143839 | TONER PROCESS - The present disclosure provides processes for increasing the shelf life and stability of resin emulsions suitable for use in forming toner particles. In embodiments, the pH of the resin emulsion is monitored, and a base is added as needed to maintain the pH of the emulsion at from about 6.5 to about 8. Maintaining the pH at from about 6.5 to about 8 prevents the degradation of the resin in the emulsion, including its molecular weight. | 06-10-2010 |
20100159387 | TONER PROCESS - The present disclosure provides processes for preparing toner particles, in which fewer coarse particles are generated. The process includes introducing a buffer solution during coalescence of the toner slurry. The amount of coarse particles in the resulting toner particles may, in embodiments, be reduced to less than about 5 percent by weight of the total toner particles generated. | 06-24-2010 |
20100186624 | METHOD OF MAKING A PIGMENTED PHASE CHANGE INK WITH DISPERSANT AND SYNERGIST - A method of making a phase change ink composition includes adding to a device with a stirring element at least one pigment, at least one dispersant and at least one synergist, processing the device at an elevated temperature and at a stirring rate to wet the at least one pigment to obtain an ink concentrate, and mixing the ink concentrate with an ink vehicle to obtain the ink composition. The device may be an extruder, an attritor or the like. The method allows for the reduction in the amount of dispersant to include in the ink. | 07-29-2010 |
20100310984 | TONER PROCESSES UTILIZING A DEFOAMER AS A COALESCENCE AID FOR CONTINUOUS AND BATCH EMULSION AGGREGATION - A process for making toner particles is provided. In embodiments, a suitable process includes adding a defoamer to an emulsion utilized to form toner particles. Utilization of the defoamer allows for a reduction in the overall aggregation/coalescence cycle time and slurry viscosity, while producing a toner with improved GSDs, low coarse and target circularities. | 12-09-2010 |
20110027712 | TONER COMPOSITIONS - The present disclosure provides toner compositions able to prevent the formation of mold or bacterial growth during storage. In embodiments, toners may include at least one biocide that prevents the formation of mold and/or bacteria in a toner composition, including any emulsion that may be utilized in forming the toner composition. In embodiments, the biocide may also improve charging characteristics of the toner. | 02-03-2011 |
20110097664 | METHOD FOR CONTROLLING A TONER PREPARATION PROCESS - A method of making toner particles, including mixing at least one emulsion of at least one resin, a colorant, an optional wax, and optional additives to form a slurry; heating the slurry to form aggregated particles in the slurry; freezing aggregation of the particles with a buffer solution; and heating the aggregated particles in the slurry to coalesce the particles into toner particles. | 04-28-2011 |
20110097665 | TONER PARTICLES AND COLD HOMOGENIZATION METHOD - A method of making toner particles, including cold homogenizing at a temperature below room temperature a resin emulsion, a colorant, an optional wax, and optional additives with a coagulant to form a toner slurry; heating the toner slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles. | 04-28-2011 |
20110129774 | INCORPORATION OF AN OIL COMPONENT INTO PHASE INVERSION EMULSION PROCESS - A process for making a resin emulsion suitable for use in forming toner particles including an oil component incorporated into the latex core of the toner particles. | 06-02-2011 |
20110136058 | EMULSION AGGREGATION METHODS - A method of making toner particles, including: mixing, at less than about 17° C. and without homogenizing, a resin emulsion with a coagulant, a colorant, an optional wax, and optional additives, to form pre-aggregated particles in a slurry; heating the slurry to form aggregated toner particles; freezing aggregation of the particles in the slurry once at a desired aggregated particle size; and further heating the aggregated particles in the slurry to coalesce the aggregated particles into toner particles. | 06-09-2011 |
20110200930 | PROCESSES FOR PRODUCING POLYESTER LATEXES VIA SOLVENT-BASED AND SOLVENT-FREE EMULSIFICATION - A process for making a latex emulsion suitable for use in a toner composition includes contacting at least one polyester resin optionally with an organic solvent to form a resin mixture, adding a primary amine, optionally a surfactant, and deionized water to the mixture. | 08-18-2011 |
20110250535 | TONER COMPOSITIONS AND PROCESSES - The present disclosure provides processes for producing polyester toners by emulsion aggregation where the resulting toner particles have high pigment loadings and desired circularity. The methods include adding a metal, in embodiments a metal compound, at the beginning of coalescence, which speeds the coalescence process and produces toner particles having a desired size and circularity for use in electrophotographic imaging systems. | 10-13-2011 |
20110281215 | PROCESSES FOR PRODUCING POLYESTER LATEXES VIA SOLVENT-BASED EMULSIFICATION - A process for making a latex emulsion suitable for use in a toner composition includes contacting at least one amorphous polyester resin with an organic solvent to form a resin mixture, adding a neutralizing agent, and deionized water to the resin mixture, removing the solvent from the formed latex, separating the solvent from water, and recycling the solvent from the resin mixture for utilization in a subsequent phase inversion emulsion process. | 11-17-2011 |
20120064453 | PROCESSES FOR PRODUCING POLYESTER LATEXES WITH IMPROVED HYDROLYTIC STABILITY - A process for making a latex emulsion suitable for use in a toner composition includes contacting at least one crystalline polyester resin with an organic solvent and a stabilizing agent to form a resin mixture, adding a neutralizing agent, and deionized water to the resin mixture, removing the solvent from the formed latex, and continuously recovering latex particles. | 03-15-2012 |
20120065359 | COLORANT-POLYESTERS AND METHODS OF PRODUCING COLORANT-POLYESTERS - An enzymatic polymerization method of covalently linking a colorant to a polyester to produce a colorant-polyester compound, the method including the steps of: (a) providing a reaction solution comprised of an ester monomer, a colorant having or functionalized to have a hydroxyl group, and an enzymatic catalyst; (b) reacting the ester monomer and the colorant using the enzymatic catalyst to produce a polymeric product, wherein the polymeric product includes a colorant-polyester compound; and (c) separating the polymeric product from the reaction solution. A colorant-polyester compound includes a colorant covalently linked to a polyester and the polyester is obtained by polymerizing a lactone. | 03-15-2012 |
20120070776 | EMULSION AGGREGATION TONERS HAVING FLOW AIDS - The present disclosure provides processes for producing toners. In embodiments, flow aids are added to a wet cake including the toner particles, prior to drying. The addition of the flow aid improves flow characteristics of the toner, thereby enhancing overall drying time, reducing the amount of coarse particles, and improving yield, without adversely affecting fusing and charging of the toner particles. | 03-22-2012 |
20120145947 | PYROPHORIC IRON NANOPARTICLES AND CONTINUOUS PROCESSES FOR PRODUCTION THEREOF - Pyrophoric nanoparticles and methods of producing the same are provided herein. An exemplary method of producing pyrophoric nanoparticles can include providing a first aqueous solution comprising at least one metal salt and an aliphatic polyether; providing a second solution comprising a metal hydride reducing agent; continuously combining the first and second solutions to produce nanoparticles in a liquid phase; separating the nanoparticles from the liquid phase; and drying the nanoparticles to form pyrophoric nanoparticles. The pyrophoric nanoparticles can have a diameter ranging from about 1 nm to about 50 nm. | 06-14-2012 |
20120156610 | TONER COMPOSITIONS AND PROCESSES - Processes for producing toners are provided. The processes include determining the desired gloss for a given toner, and determining the desired amount of aluminum in the toner to obtain that gloss. Utilizing the processes of the present disclosure, the solids content of an emulsion utilized to produce such a toner, as well as the mixing speed utilized in the aggregation process and the temperature at which aggregation of the toner particles occurs, may then be selected to obtain toner particles possessing the desired amount of aluminum, and thus the desired gloss. | 06-21-2012 |
20120202148 | Emulsion Aggregation Toner Compositons - Disclosed is a toner which comprises particles comprising: (a) a core comprising: (1) a first resin; and (2) a first conductive colorant; and (b) a shell comprising: (1) a second resin; and (2) a second conductive colorant. | 08-09-2012 |
20120231386 | TONER PARTICLES COMPRISING COLORANT-POLYESTERS - A toner composition including a colorant-polyester polymer having at least one colorant and at least one polyester resin, an optional non-colorant polyester polymer, an optional additional colorant, an optional wax, and an optional additive, where the colorant is covalently linked to some or all of the polyester resin and the polyester resin is obtained by polymerizing a lactone using an enzyme catalyst. Methods for preparing a toner composition including an emulsion aggregation process. | 09-13-2012 |
20120258393 | CO-EMULSIFICATION OF INSOLUBLE COMPOUNDS WITH TONER RESINS - A process for making a latex emulsion suitable for use in a toner composition includes co-emulsifying a bio-based resin with an insoluble component, such as a pigment or wax, whereby the resin encapsulates the insoluble component. The resulting latex, including the insoluble component encapsulated in the resin, may then be utilized to form a toner. The insoluble component may thus be included in toner particles, which might otherwise be difficult to achieve, using emulsion aggregation processes. | 10-11-2012 |
20120258397 | CO-EMULSIFICATION OF INSOLUBLE COMPOUNDS WITH TONER RESINS - A process for making a latex emulsion suitable for use in a toner composition includes co-emulsifying a bio-based resin with an insoluble component, such as a pigment or wax, whereby the resin encapsulates the insoluble component. The resulting latex, including the insoluble component encapsulated in the resin, may then be utilized to form a toner. The insoluble component may thus be included in toner particles, which might otherwise be difficult to achieve, using emulsion aggregation processes. | 10-11-2012 |
20120308925 | Hyperpigmented black low melt toner - The present disclosure describes a hyperpigmented low melt black toner containing a thermal carbon black which exhibits reduced dielectric loss and improved tribo charging. | 12-06-2012 |
20130122418 | Alkyl Benzene Sulfonate Surfactant Having An Ammonium Salt Counter Ion For Reduced Sodium Content In Emulsions - A process including contacting an alkyl benzene sulfonate surfactant having an ammonium salt counter ion with a component to be emulsified or dispersed, wherein the alkyl benzene sulfonate surfactant is substantially free of sodium salt counter ions such that the sodium content of the alkyl benzene sulfonate surfactant is less than about 5,000 parts per million, and water to form a mixture; using the alkyl benzene sulfonate surfactant to emulsify the component and form an emulsion; or using the alkyl benzene sulfonate surfactant to disperse the component and form a dispersion. | 05-16-2013 |
20140170548 | Continuous Production of Toner - Continuous and semi-continuous emulsion aggregation processes for the production of toner particles are presented. | 06-19-2014 |
20140170557 | Batch/Continuous Production of Toner - A process for forming toner using an emulsion/aggregation scheme wherein particle aggregation occurs in a batch reactor and coalescence occurs in a continuous reactor, with a space time yield of at least 200 g/L/hr. | 06-19-2014 |
20140170558 | Batch/Continuous Production of Toner - A process for forming toner using an emulsion/aggregation scheme wherein particle aggregation occurs in a batch reactor and coalescence occurs in a continuous reactor. In embodiments, a continuous reactor comprises four sections joined in series. | 06-19-2014 |
20140199625 | Preparing Amorphous Polyester Resin Emulsions - A process for making a latex emulsion including contacting at least one amorphous polyester resin with at least two organic solvents to form a resin mixture, adding a neutralizing agent, and deionized water to the resin mixture, removing the solvent from the formed latex, and separating the solvent from water. Further, the process is carried out above the resin Tg for making the latex, which drives the latex particle size under 100 nm, where toners made from the latex show improved charging performance. | 07-17-2014 |
20140248558 | Preparing Colorant Dispersions Using Acoustic Mixing - The present disclosure provides processes for making inorganic or organic colorant dispersions using an acoustic mixer, where such dispersion may be used to make toner. Such processes apply low frequency, high intensity acoustic energy and a consistent shear field throughout an entire mixing vessel and provide uniform dispersion of colorants within minutes. | 09-04-2014 |